Acid Etching as Surface Treatment Method for Luting of Glass-Ceramic Restorations, part 1: Acids, Application Protocol and Etching Effectiveness
DOI:
https://doi.org/10.3889/oamjms.2018.147Keywords:
Acid etching, Ceramic surface treatment, Hydrofluoric acid, Acidulated phosphate fluoride, Ammonium hydrogen bifluorideAbstract
AIM: The purpose of this review is to represent acids that can be used as surface etchant before adhesive luting of ceramic restorations, placement of orthodontic brackets or repair of chipped porcelain restorations. Chemical reactions, application protocol, and etching effect are presented as well.
STUDY SELECTION: Available scientific articles published in PubMed and Scopus literature databases, scientific reports and manufacturers' instructions and product information from internet websites, written in English, using following search terms: “acid etching, ceramic surface treatment, hydrofluoric acid, acidulated phosphate fluoride, ammonium hydrogen bifluorideâ€, have been reviewed.
RESULTS: There are several acids with fluoride ion in their composition that can be used as ceramic surface etchants. The etching effect depends on the acid type and its concentration, etching time, as well as ceramic type. The most effective etching pattern is achieved when using hydrofluoric acid; the numerous micropores and channels of different sizes, honeycomb-like appearance, extruded crystals or scattered irregular ceramic particles, depending on the ceramic type, have been detected on the etched surfaces.
CONCLUSION: Acid etching of the bonding surface of glass - ceramic restorations is considered as the most effective treatment method that provides a reliable bond with composite cement. Selective removing of the glassy matrix of silicate ceramics results in a micromorphological three-dimensional porous surface that allows micromechanical interlocking of the luting composite.Downloads
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References
Pameijer CH. A review of luting agents. Int J Dent. 2012; 2012:752861. https://doi.org/10.1155/2012/752861 PMid:22505909 PMCid:PMC3296365
Diaz-Arnold A, Vargas MA, Haselton DR. Current status of luting agents for fixed prosthodontics. J Prosthet Dent. 1999; 81:135-41. https://doi.org/10.1016/S0022-3913(99)70240-4
Krämer N, Lohbauer U, Frankenberger R. Adhesive luting of indirect restorations. Am J Dent. 2000; 13:60D-76D. PMid:11763920
Chen L, In Suh B. Bonding of resin materials to all-ceramics: a review. Current research in dentistry. 2012; 3:7-17. https://doi.org/10.3844/crdsp.2012.7.17
Blatz MB, Sadan A, Kern M. Resin-ceramic bonding: a review of the literature. J Prosthet Dent. 2003; 89:268-74. https://doi.org/10.1067/mpr.2003.50 PMid:12644802
Vargas MA, Bergeron C, Diaz-Arnold A. Cementing all-ceramic restorations. JADA. 2011; 142:20S-4S. https://doi.org/10.14219/jada.archive.2011.0339 PMid:21454837
Burke FJ, Fleming GJ, Nathanson D, Marquis PM. Are adhesive technologies needed to support ceramics? An assessment of the current evidence. J Adhes Dent. 2002; 4:7-22. PMid:12071631
Ho GW, Matinlinna JP. Insights on ceramics as dental materials. Part II: chemical surface treatments. Silicon. 2011; 3:117-23. https://doi.org/10.1007/s12633-011-9079-6
Borges GA, Sophr AM, de Goes MF, Sobrinho C, Chan DCN. Effect of etching and airborne particle abrasion on the microstructure of different dental ceramics. J Prosthet Dent. 2003; 89:479-88. https://doi.org/10.1016/S0022-3913(02)52704-9
Matinlinna JP, Lassila LV, Özcan M, Yli-Urpo A, Vallittu PK. An introduction to silanes and their clinical applications in dentistry. Int J Prosthodont. 2004; 17:155-64. PMid:15119865
Lung CYK, Matinlinna JP. Aspects of silane coupling agents and surface conditioning in dentistry: An overview. Dent Mater. 2012; 28:467-77. https://doi.org/10.1016/j.dental.2012.02.009 PMid:22425571
Lung CYK, Kukk E, Hägerth T, Matinlinna JP. Surface modification of silica-coated zirconia by chemical treatments. Appl Surf Sci. 2010; 257:1228-35. https://doi.org/10.1016/j.apsusc.2010.08.029
Inokoshi M, Kameyama A, De Munck J, Minakuchi S, Van Meerbeek B. Durable bonding to mechanically and/or chemically pre-treated dental zirconia. J Dent. 2013; 41:170-9. https://doi.org/10.1016/j.jdent.2012.10.017 PMid:23137995
Bottino MC, Özcan M, Coelho PG, Valandro LF, Bressiani JC, Bressiani AHA. Micro-morphological changes prior to adhesive bonding: high-alumina and glassy-matrix ceramics. Braz Oral Res. 2008; 22:158-63. https://doi.org/10.1590/S1806-83242008000200011 PMid:18622486
Aboushelib MN, Kleverlaan CJ, Feilzer AJ. Selective infiltration-etching technique for a strong and durable bond of resin cements to zirconia-based materials. J Prosthet Dent. 2007; 98:379-88. https://doi.org/10.1016/S0022-3913(07)60123-1
Casucci A, Mazzitelli C, Monticelli F, Toledano M, Osorio R, Osorio E, Papacchini F, Ferrari M. Morphologycal analysis of three zirconium oxide ceramics: Effect of surface treatments. Dent Mater. 2010; 26:751-60. https://doi.org/10.1016/j.dental.2010.03.020 PMid:20471073
Aboushelib MN, Matinlinna JP, Salameh Z, Ounsi H. Innovations in bonding to zirconia-based materials: part I. Dent Mater. 2008; 24:1268-72. https://doi.org/10.1016/j.dental.2008.02.010 PMid:18417204
Aboushelib MN, Feilzer AJ, Kleverlaan CJ. Bonding to zirconia using a new surface treatment. J Prosthodont. 2010; 19:340-6. https://doi.org/10.1111/j.1532-849X.2010.00575.x PMid:20202104
Piascik JR, Swift EJ, Thompson JY, Grego S, Stoner BR. Surface modification for enhanced silanation of zirconia ceramics. Dent Mater. 2009; 25:1116-21. https://doi.org/10.1016/j.dental.2009.03.008 PMid:19376572 PMCid:PMC2720441
Hallmann L, Ulmer P, Wille S, Polonskyi O, Köbel S, Trottenberg T, Bornholdt S, Haase F, Kersten H, Kern M. Effect of surface treatments on the properties and morphological change of dental zirconia. J Prosthet Dent. 2016; 115:341-9. https://doi.org/10.1016/j.prosdent.2015.09.007 PMid:26581661
Hallmann L, Ulmer P, Lehmann F, Wille S, Polonskyi O, Johannes M, Köbel S, Trottenberg T, Bornholdt S, Haase F, Kersten H, Kern M. Effect of surface modifications on the bond strength of zirconia ceramic with resin cement resin. Dent Mater. 2016; 32:631-9. https://doi.org/10.1016/j.dental.2016.02.001 PMid:26898723
Valverde GB, Coelho PG, Janal MN, Lorenzoni FC, Carvalho RM, Thompson VP et al. Surface characterization and bonding of Y-TZP following non-thermal plasma treatment. J Dent. 2013; 41(1):51-9. https://doi.org/10.1016/j.jdent.2012.10.002 PMid:23044388
Jevnikar P, Krnel K, Kocjan A, Funduk N, Kosmac T. The effect of nano-structured alumina coating on resin-bond strength to zirconia ceramics. Dent Mater. 2010; 26(7):688-96. https://doi.org/10.1016/j.dental.2010.03.013 PMid:20381854
Külünk T, Külünk Ş, Baba S, Öztürk Ö, Danişman Ş, Savaş S. The effect of alumina and aluminium nitride coating by reactive magnetron sputtering on the resin bond strength to zirconia core. J Adv Prosthodont. 2013; 5(4):382-7. https://doi.org/10.4047/jap.2013.5.4.382 PMid:24353874 PMCid:PMC3865191
Özcan M, Vallittu PK. Effect of surface conditioning methods on the bond strength of luting cement to ceramics. Dent Mater. 2003; 19:725-31. https://doi.org/10.1016/S0109-5641(03)00019-8
Peumans M, Valjakova EB, De Munck J, Mishevska CB, Van Meerbeek B. Bonding effectiveness of luting composites to different CAD/CAM materials. J Adhes Dent. 2016; 18(4):289-302. PMid:27222889
Simonsen RJ, Calamia JR. Tensile bond strength of etched porcelain. J Dent Res. 1983; 62:297; Abstr. No. 1154.
Yen TY, Blackman RB, Baez RJ. J. Effect of acid etching on the flexural strength of a feldspathic porcelain and a castable glass ceramic. J Prosthet Dent. 1993; 70:224-33. https://doi.org/10.1016/0022-3913(93)90056-T
http://www.ivoclarvivadent.us/zoolu-website/media/document/4176/IPS+Ceramic +Etching+ gel+ (document last reviewed on 04/14/2016). Accessed May 1, 2016.
https://www.vita-zahnfabrik.com/en/VITA-CERAMICS-ETCH-26710,27568.html. Accessed May 1, 2016.
https://www.ultradent.com/en-us/Dental-Products-Supplies/Bond-Etch/Etchants/ Hydrofluoric-Acid-Gel/Ultradent-Porcelain-Etch-and-Silane-Ceramic-Etchant-and-Silane-Solution/Pages/default.aspx. Accessed May 1, 2016.
https://www.bisco.com/instructions/%284%29Porcelain%20Etchant_English.pdf. Accessed May 1, 2016.
https://www.bisco.com/instructions/%289.5%29Porcelain%20Etchant_English.pdf. Accessed May 1, 2016.
http://www.miragecdp.com/por_etch.htm. Accessed May 1, 2016.
http://www.ivoclarvivadent.us/zoolu-website/media/document/16985/ IPS+Ceramic+Etching +gel+. Accessed May 1, 2016.
Bajraktarova Valjakova E. [Evaluation of the bonding effectiveness of luting composites to different ceramic CAD/CAM materials – in vitro study] [dissertation]. Faculty of Dentistry, University "Ss Cyril and Methodius"; 2014. Macedonian.
Bajraktarova Valjakova E, De Munck J, Yoshihara K, Misevska C, Grozdanov A, Peumans M, Van Meerbeek B. Micro-morphological changes of various CAD-CAM blocks after different surface treatments. 47th Meeting of CED-IADR, Antalya, Turkey; 2015. Abstr. No. 0576.
Scheller-Sheridan C. Acid etchant, bonding agents and fissure sealants. In: Scheller-Sheridan C, editor. Basic guide to dental materials, 1st ed., Oxford, UK: Wiley-Blackwell, 2010:63-79.
Della Bona A. Characterizing ceramics and the interfacial adhesion to resin: II- the relationship of surface treatment, bond strength, interfacial toughness and fractography. J Appl Oral Sci. 2005; 13:101-9. https://doi.org/10.1590/S1678-77572005000200002 PMid:20924531
Matinlinna JP, Vallittu PK. Bonding of resin composites to etchable ceramic surfaces - an insight review of the chemical aspects on surface conditioning. J Oral Rehabil. 2007; 34(8):622-30. https://doi.org/10.1111/j.1365-2842.2005.01569.x PMid:17650173
Van Noort R. All-ceramic restorations: resin-bonded ceramics. In: Van Noort R, editor. Introduction to dental materials, 3rd ed., Philadelphia, PA: Elsevier, 2007: 261-9.
Aida M, Hayakawa T, Mizukawa K. Adhesion of composite porcelain with various surface conditions. J Prosthet Dent. 1995; 73(5):464-70. https://doi.org/10.1016/S0022-3913(05)80076-9
Della Bona A, Anusavice KJ. Microstructure, composition, and etching topography of dental ceramics. Int J Prosthodont. 2002; 15(2):159-67. PMid:11951806
Canay Åž, Hersek N, Ertan A. Effect of different acid treatments on a porcelain surface. J Oral Rehabil. 2001; 28(1):95-101. https://doi.org/10.1046/j.1365-2842.2001.00626.x PMid:11298915
Della Bona A, Anusavice KJ, Hood JA. Effect of ceramic surface treatment on tensile bond strength to a resin cement. Int J Prosthodont. 2002; 15(3):248-53. PMid:12066487
Ccahuana VZS, Özcan M, Mesquita AMM, Nishioka RS, Kimpara ET, Bottino MA. Surface degradation of glass ceramics after exposure to acidulated phosphate fluoride. J Appl Oral Sci. 2010; 18(2):155-65. https://doi.org/10.1590/S1678-77572010000200010 PMid:20485927 PMCid:PMC5349752
Kato H, Matsumura H, Atsuta M. Effect of etching and sandblasting on bond strength to sintered porcelain of unfilled resin. J Oral Rehabil. 2000; 27(2):103-10. https://doi.org/10.1046/j.1365-2842.2000.00489.x PMid:10672145
Kukiattrakoon B, Thammasitboon K. The effect of different etching times of acidulated phosphate fluoride gel on the shear bond strength of high-leucite ceramics bonded to composite resin. J Prosthet Dent. 2007; 98(1):17-23. https://doi.org/10.1016/S0022-3913(07)60033-X
Addison O, Marquis PM, Fleming GJP. The impact of hydrofluoric acid surface treatments on the performance of a porcelain laminate restorative material. Dent Mater. 2007; 23(4):461-8. https://doi.org/10.1016/j.dental.2006.03.002 PMid:16620948
Stangel I, Nathanon D, Hsu CS. Shear strength of the composite bond to etched porcelain. J Dent Res. 1987; 66(9):1460-5. https://doi.org/10.1177/00220345870660091001 PMid:3305639
Wolf DM, Powers JM, O'Keefe KL. Bond strength of composite to etched and sandblasted porcelain. Am J Dent. 1993; 6(3):155-8.
PMid:8240779
Zogheib LV, Della Bona A, Kimpara ET, McCabe JF. Effect of hydrofluoric acid etching duration on the roughness and flexural strength of a lithium disilicate-based glass ceramic. Braz Dent J. 2011; 22(1):45-50. https://doi.org/10.1590/S0103-64402011000100008 PMid:21519648
Chen JH, Matsumura H, Atsuta M. Effect of different etching periods on the bond strength of a composite resin to a machinable porcelain. J Dent. 1998; 26(1):53-8. https://doi.org/10.1016/S0300-5712(96)00078-4
Nagayassu MP, Shintome LK, Uemura ES, de Araujo JEJ. Effect of surface treatment on the shear bond strength of a resin-based cement to porcelain. Braz Dent J. 2006; 17(4):290-5. https://doi.org/10.1590/S0103-64402006000400005 PMid:17262141
Kim B-K, Bae H E-K, Shim J-S, Lee K-W. The influence of ceramic surface treatments on the tensile bond strength of composite resin to all-ceramic coping materials. J Prosthet Dent. 2005; 94(4):357-62. https://doi.org/10.1016/j.prosdent.2005.08.012 PMid:16198173
Valandro LF, Della Bona A, Antonio Bottino M, Neisser MP. The effect of ceramic surface treatment on bonding to densely sintered alumina ceramic. J Prosthet Dent. 2005; 93(3):253-9. https://doi.org/10.1016/j.prosdent.2004.12.002 PMid:15775926
Lu YC, Tseng H, Shin YH, Lee SY. Effects of surface treatments on bond strength of glass-infiltrated ceramic. J Oral Rehabil. 2001; 28(9):805-13. https://doi.org/10.1046/j.1365-2842.2001.00735.x
Özcan M, Alkumru HN, Gemalmaz D. The effect of surface treatment on the shear bond strength of luting cement to a glass-infiltrated alumina ceramic. Int J Prosthodont. 2001; 14(4):335-9. PMid:11508088
Kern M, Wegner SM. Bonding to zirconia ceramic: Ahesion methods and their durability. Dent Mater. 1998; 14(1):64-71. https://doi.org/10.1016/S0109-5641(98)00011-6
Derand P, Derand T. Bond strength of luting cements to zirconium oxide ceramics. Int J Prosthodont. 2000; 13(2):131-5. PMid:11203621
Della Bona A, Anusavice KJ, Shen C. Microtensile strength of composite bonded to hot-pressed ceramics. J Adhes Dent. 2000; 2(4):305-13. PMid:11317377
Madani M, Chu FCS, McDonalds AV, Smales RJ. Effects of surface treatments on shear bond strengths between a resin cement and an alumina core. J Prosthet Dent. 2000; 83(6):644-7. https://doi.org/10.1067/mpr.2000.107337 PMid:10842131
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